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The Analytical Scientist / Issues / 2025 / June / Spectroscopy Roundup: Palm Oil Fraud, Tumor Clues, and Lunar Glass
Spectroscopy Materials Science News and Research

Spectroscopy Roundup: Palm Oil Fraud, Tumor Clues, and Lunar Glass

Recent research – from food authentication to real-time cancer diagnostics and the Moon’s volcanic past

06/24/2025 5 min read

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0625-103-Spec-News_Teaser.png (1)

This image shows a detailed, thousand-colour image of the Sculptor Galaxy captured with the MUSE instrument at ESO’s Very Large Telescope (VLT). Regions of pink light are spread throughout this whole galactic snapshot, which come from ionised hydrogen in star-forming regions. These areas have been overlaid on a map of already formed stars in Sculptor to create the mix of pinks and blues seen here. Credit: ESO/E. Congiu et al.

Portable Raman Shines Light on Palm Oil Provenance

A new study showcases the power of handheld Raman spectroscopy to trace the geographic origin of palm oil – offering a fast, non-destructive solution to long-standing challenges in food fraud and sustainability oversight.

Focusing on samples from Ghana and the Ivory Coast, researchers led by Roy Goodacre used portable Raman devices paired with chemometric analysis to distinguish palm oils by their β-carotene content – a natural pigment linked to geographic origin and fruit maturity. Principal component analysis (PCA) and partial least squares regression (PLS-R) revealed that β-carotene levels correlated strongly with both location and colour differences in oil samples. Even when some oils appeared unusually light in colour, NMR spectroscopy confirmed their identity as palm oil rather than palm kernel oil – highlighting cases where synthetic dyes may have been used to manipulate appearance.

By identifying distinct spectral signatures tied to different regions and producers, this method could support enforcement against mislabelling and deforestation-linked production, while giving consumers greater confidence in certified sustainable palm oil claims.

A Thousand Colors, One Galaxy: Sculptor Revealed in Unprecedented Detail

Astronomers have created the most detailed map yet of the Sculptor Galaxy (NGC 253), capturing thousands of spectral fingerprints across its sprawling disk and uncovering a trove of new planetary nebulae. Using over 50 hours of observations with the MUSE instrument on ESO’s Very Large Telescope, the team stitched together a full-spectrum mosaic, revealing the age, motion, and composition of stars and gas in unprecedented detail.

Unlike conventional images limited to a handful of colors, this “galaxy in a thousand colors” shows the Sculptor’s complex structure through its light – from newborn stars in pink, hydrogen-rich regions to ancient stellar populations and gas clouds. The dataset enabled researchers to detect nearly 500 planetary nebulae, ten times more than typically observed in similar galaxies, providing precise distance measurements and valuable insights into galactic evolution.

“We can zoom in to study star-forming regions almost at the scale of individual stars, and zoom out to analyze the galaxy as a whole,” said co-author Kathryn Kreckel in a press release.

Smarter, Faster Liver Tumor Diagnosis in the OR

A new study demonstrates that fiber-based attenuated total reflection infrared (ATR IR) spectroscopy, combined with machine learning, can classify liver tumors with 90 percent accuracy – offering a fast, objective alternative to traditional frozen section analysis during surgery. The method relies on distinctive molecular signatures captured via IR spectra, particularly glycogen and protein content, to distinguish between normal tissue and tumor subtypes including hepatocellular carcinoma (HCC), cholangiocellular carcinoma (CCC), and metastases.

In the study, fresh resection samples from 69 patients were analyzed using a Ge crystal ATR probe and silver halide fibers. Key spectral differences were found in glycogen-rich regions, with HCC showing the highest glycogen levels and CCC displaying stronger protein-associated signatures. The algorithm was trained on supervised classification models and validated with an independent test set, achieving high sensitivity and specificity.

This real-time, label-free method could enhance intraoperative decision-making, reduce recurrence risks, and may be adaptable for use in other solid tumors.

Bacterial Bandits: Pandoraea’s Iron-Snatching Tactics Revealed

In a deep dive into the survival strategies of the rare and resistant Pandoraea genus, scientists have discovered two potent natural compounds – Pandorabactin A and B – that allow these pathogens to outcompete rivals by stealing iron. Detailed in Angewandte Chemie, the molecules were uncovered through bioinformatics, gene knockout studies, and structural analysis using mass spectrometry and NMR.

Encoded by the previously unknown pan gene cluster, the compounds are siderophores – iron-chelating agents that give Pandoraea an edge in nutrient-starved environments like the human lung. In lab assays, Pandorabactins starved out other bacteria including Pseudomonas and Mycobacterium, while clinical sputum samples from cystic fibrosis patients showed the pan gene’s presence coinciding with shifts in lung microbiome composition.

“The molecules help the bacteria to take up iron when it is scarce in their environment,” said Elena Herzog, first author of the study in a press release. Though too early for clinical translation, the work sheds light on a stealthy microbial tactic with potential implications for infection dynamics and microbiome modulation.

Volcanic Glass Beads Reveal Explosive Secrets of the Moon’s Fiery Youth

Tiny orange and black glass beads collected by Apollo astronauts have provided a rare glimpse into the Moon’s explosive volcanic history, thanks to cutting-edge analytical techniques that examine their surface chemistry and formation. A study published in Icarus uses high-resolution spectroscopic methods to decode the mineral makeup of these ancient droplets, which formed during fire fountain–style eruptions over 3.3 billion years ago.

Researchers from Brown University, Washington University in St. Louis, and collaborators employed a powerful toolkit of microanalytical techniques: NanoSIMS (nanoscale secondary ion mass spectrometry) to detect isotopic and elemental surface signatures, atom probe tomography to reconstruct three-dimensional atomic structure, scanning and transmission electron microscopy (SEM/TEM) for nanoscale imaging, and energy dispersive X-ray spectroscopy (EDS) for elemental mapping. These tools revealed mineral nanocrystals – particularly zinc sulfides – condensed from sulfur-rich volcanic vapors, differing between orange and black beads in a way that tracks changes in eruption chemistry and redox conditions over time.

“We’ve had these samples for 50 years, but we now have the technology to fully understand them,” said physicist Ryan Ogliore of WashU in a press release. “Each bead tells a story.”

The findings show how eruption style on the Moon evolved and highlight the beads as pristine time capsules of early lunar volcanism – capturing not only the violence of the Moon’s past, but its deep interior composition and volatile history.

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